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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1649733Generated: November 2, 2026

Benzoyl chloride → 120067-47-2

https://huagongshe.com/reaction/1649733

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoyl chlorideHCID 7412—
ReactantHydrocarbostyrilHCID 64796—
ReactantAluminum(III) ChlorideHCID 6451240—
SolventCarbon DisulfideHCID 6348—
Product120067-47-2HCID 14373255—

Reaction Steps

A mixture of 2.2 g of 3,4-dihydrocarbostyril, 3.21 g of benzoyl chloride and 13 g of aluminum chloride in 50 ml of carbon disulfide was refluxed for 2 days. The reaction mixture was poured onto ice water and the resulting solid filtered off, washed with water and dried under reduced pressure to yield 6-benzoyl-3,4-dihydrocarbostyril, m.p. 205°-207° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04921862
Source datasetuspto-grants-1990_05
ORD IDord-e27d9f1b58714320bc123bbc0b2fe8b0
Source noteuspto-grants-1990_05