HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyridine → HCID 14373283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | 6-ethynyl-3,4-dihydroquinolin-2(1H)-one | HCID 14373291 | — |
| Catalyst | Dichlorobis(triphenylphosphine)palladium | HCID 6102075 | — |
| Product | HCID 14373283 | HCID 14373283 | — |
Reaction Steps
A mixture of 11.6 mg of cuprous iodide, 86 mg of bis (triphenylphosphine)palladium(II)dichloride, 1.0 g of 6-ethynyl-3,4-dihydrocarbostyril and 3-bromopyridine were reacted as shown in Example 9, and the product isolated in a similar fashion, giving 6-[2-(3-pyridyl)ethynyl]-3,4-dihydrocarbostyril, m.p. 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04921862 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-46ba0e46ddb04e44ac47013c5f00cd58 |
| Source note | uspto-grants-1990_05 |