HRID1649744

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12286

3-Bromopyridine

C5H4BrN

HCID14373291

未命名化合物

PRODUCTS

生成物

HCID14373283

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

结构：[Cl][Pd][Cl].c1ccc(P(c2ccccc2)c2ccccc2)cc1.c1ccc(P(c2ccccc2)c2ccccc2)cc1

催化剂HCID6102075

未命名化合物

PROCEDURE

实验过程

A mixture of 11.6 mg of cuprous iodide, 86 mg of bis (triphenylphosphine)palladium(II)dichloride, 1.0 g of 6-ethynyl-3,4-dihydrocarbostyril and 3-bromopyridine were reacted as shown in Example 9, and the product isolated in a similar fashion, giving 6-[2-(3-pyridyl)ethynyl]-3,4-dihydrocarbostyril, m.p. 195°-197° C.

WORKUP

后处理

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