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HRID1649789

反应详情

EQUATION

反应方程式

HRID 1649789 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(Br)nc1
HCID78240

2-Bromo-5-nitropyridine

C5H3BrN2O2

结构：C#CCOCCCCCCBr
HCID21895501

1-Bromo-6-[(prop-2-yn-1-yl)oxy]hexane

C9H15BrO

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(C#CCOCCCCCCBr)nc1
HCID19854800

未命名化合物

PROCEDURE

实验过程

2-Bromo-5-nitropyridine (6.4 g) and 1-bromo-6-[(2-propynyl)oxy]hexane (6.39 g) were treated as in Intermediate 20 to give, after FCC eluting with hexane-ether (2:1), the title compound as a brown oil (7 g), t.l.c. (hexane-ether 5:1) Rf 0.22.

WORKUP

后处理

  1. customto give
  2. washafter FCC eluting with hexane-ether (2:1)