HCID 13674870, compound → HCID 13674809, compound

Participants

Reaction Steps

A solution of 0.2 g (0.8 mmoles) of 1-(N-ethyl-acetamido)-2(2,6-dimethylphenyl-amino)-propane, prepared as described in Example 31, in 5 ml of dry diethyl ether is added dropwise, within 10 minutes, to a vigorously stirred suspension of 0.2 g of lithium aluminium hydride in 10 ml of dry diethyl ether at room temperature. The resulting mixture is stirred at room temperature for 3 hours and then processed as described in Example 29. 0.14 g (74%) of 1-diethylamino-2-(2,6-dimethylphenyl-amino)-propane are obtained.

Provenance & Evidence