2,6-Dimethylaniline → HCID 13674869, compound

HRID 1649997Notes

Reaction equation

HRID 1649997 reaction equation
[CH3:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:5]([CH3:9])[C:3]=1[NH2:4].[CH3:10][N:11]([CH2:14][CH:15](Cl)[CH3:16])[CH:12]=[O:13]>>[CH3:10][N:11]([CH2:14][CH:15]([NH:4][C:3]1[C:5]([CH3:9])=[CH:6][CH:7]=[CH:8][C:2]=1[CH3:1])[CH3:16])[CH:12]=[O:13]

Participants

3

Reactant 2

HCID 68962,6-DimethylanilineHCID 13674867HCID 13674867, compound

Product 1

HCID 13674869HCID 13674869, compoundYield 22%

Procedure

One proceeds as described in Method C) of Example 14 with the difference that 2,6-dimethyl-aniline and 1-(N-methylformamido)-2-chloro-propane are applied as starting substances. The title compound is obtained with a yield of 22%; b.p.: 155°-165° C./80 Pa, m.p.: 69.5°-72° C.

Sources & evidence

ORD record
ord-74831b4612d148fbb1565073b1bb675c
Source dataset
uspto-grants-1990_05
Patent number
US04922021

Reaction notes

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