Hydrochloric Acid → HCID 19855586, compound

HRID 1650004Notes

Reaction equation

HRID 1650004 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[N:9]([CH2:14][CH:15]([NH:17][CH2:18][CH2:19]O)[CH3:16])[S:10]([CH3:13])(=[O:12])=[O:11].[ClH:21]>>[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[N:9]([CH2:14][CH:15]([NH:17][CH2:18][CH2:19][Cl:21])[CH3:16])[S:10]([CH3:13])(=[O:12])=[O:11]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 13674840HCID 13674840, compound

Product 1

HCID 19855586HCID 19855586, compoundYield 87%

Procedure

The title compound is prepared as described in Example 50, with the difference that 1-[N-(2,6-dimethylphenyl)-methane-sulfonamido]-2-(2-hydroxy-ethylamino)-propane, prepared according to Example 46, is applied as starting substance. The product is obtained with a yield of 87%; its hydrochloride melts at 185°-190° C.

Workup

  1. customprepared
  2. customThe product is obtained with a yield of 87%

Sources & evidence

ORD record
ord-3a563a8303344698b6915dfb3f843c74
Source dataset
uspto-grants-1990_05
Patent number
US04922021

Reaction notes

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