HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23043913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Cyclohexylethylamine | HCID 20509 | — |
| Reactant | Methyl 6-chloro-6-oxohexanoate | HCID 520737 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23043913 | HCID 23043913 | — |
Reaction Steps
Methyl 5-[chloroformyl]pentanoate (4.2 g) in dry dichloromethane (20 ml) was added dropwise to a stirred solution of 2-cyclohexylethylamine (3 g) and triethylamine (3.3 ml) in dry dichloromethane (40 ml) under a N2 atmosphere. The mixture was stirred at room temperature for 16 hours and heated under reflux for 1.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04922022 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-358b0f73fe0949889373bf715257652f |
| Source note | uspto-grants-1990_05 |