HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → (3-Vinylphenyl)phenylmethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | HCID 178436337 | HCID 178436337 | — |
| Product | (3-Vinylphenyl)phenylmethane | HCID 14882414 | — |
Reaction Steps
The method using benzyl chloride as a starting material is described. Benzyl chloride is reacted with a Grignard reagent of 3-vinylphenylmagnesium bromide in the presence of dichlorodiphosphine nickel complex catalyst to obtain (3-vinylphenyl)phenylmethane. The reaction temperature using Grignard reagent is in the range of 10° to 80° C. and the use quantity of Grignard reagent is 1.0 to 1.2 equivalent to 1 mole of benzyl chloride. ##STR8##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04922052 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-08e16c81b8a3422796d0dce2f123f552 |
| Source note | uspto-grants-1990_05 |