Hydrochloric Acid → FK 336

HRID 1650189Notes

Reaction equation

HRID 1650189 reaction equation
[N+:1]([O:4][CH2:5][CH2:6][NH:7][C:8]([C:10]1[N:11]=[C:12]([CH3:15])[S:13][CH:14]=1)=[O:9])([O-:3])=[O:2].[ClH:16]>>[ClH:16].[N+:1]([O:4][CH2:5][CH2:6][NH:7][C:8]([C:10]1[N:11]=[C:12]([CH3:15])[S:13][CH:14]=1)=[O:9])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 1294034-Thiazolecarboxamide, 2-methyl-N-[2-(nitrooxy)ethyl]-

Product 1

HCID 129402FK 336

Procedure

N-(2-Nitrooxyethyl)-2-methyl-4-thiazolecarboxamide was transformed into its hydrochloride in a conventional manner, followed by recrystallization from ethanol to obtain white crystals of N-(2-nitrooxyethyl)-2-methyl-4-thiazolecarboxamide hydrochloride.

Workup

  1. customfollowed by recrystallization from ethanol

Sources & evidence

ORD record
ord-0606c13a7f0c41f6aa162879669df6f6
Source dataset
uspto-grants-1990_05
Patent number
US04923886

Reaction notes

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