HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetic Acid → N-Phenylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetic Acid | HCID 300 | — |
| Reactant | Aniline | HCID 6115 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-Phenylglycine | HCID 66025 | — |
Reaction Steps
475 g (5 mols) of chloroacetic acid are heated at 100° C. with 930 g (10 mols) of aniline in 2 l. of water for 1.5 hours. After the mixture has been cooled, the N-phenylglycine formed is filtered off with suction and washed with water. Yield: 468 g (=62%, relative to the chloroacetic acid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04924004 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-07c94b3e452e4a63aa7beb2bdf8725e7 |
| Source note | uspto-grants-1990_05 |