Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1650618Generated: November 3, 2026

Thionyl Chloride → HCID 19762694, compound

https://huagongshe.com/reaction/1650618

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 18371174HCID 18371174—
ProductHCID 19762694HCID 19762694100%

Reaction Steps

1.24g (5 mmoles) of 3-(1-methylcyclohexyl)-4-methoxybenzoic acid and 15 ml of thionyl chloride are heated at reflux until the cessation of gas evolution. The reaction mixture is evaporated to dryness. 1.32 g (100% yield) of crude 3-(1-methylcyclohexyl)-4-methoxybenzoic acid chloride which is used as such for the following synthesis are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04925658
Source datasetuspto-grants-1990_05
ORD IDord-f675b0cadf4040afaee461fe293f2b57
Source noteuspto-grants-1990_05