Stearoyl chloride → Palmitoyl chloride

HRID 1650663Notes

Reaction equation

HRID 1650663 reaction equation
CC1N(CCC2CCNCC2)C=CN=1.[C:15]([Cl:34])(=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30]CC>>[C:15]([Cl:34])(=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]

Participants

3

Reactant 2

HCID 8212Stearoyl chlorideHCID 64846854-[2-(2-Methyl-1H-imidazol-1-yl)ethyl]piperidine

Product 1

HCID 8206Palmitoyl chloride

Procedure

Following essentially the last step of the procedure for preparing the compound of Example 1, and using in place of stearoyl chloride, an approximately equivalent amount of hexadecanoyl chloride, the title compound was obtained, m.p. 112° to 115° C.

Sources & evidence

ORD record
ord-67a99a79d1d84d7a84581ed1757fb2d1
Source dataset
uspto-grants-1990_05
Patent number
US04925851

Reaction notes

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