HCID 23052546, compound → HCID 23052545, compound

Participants

Reaction Steps

41 g of 2,5-dichloro-4-pentafluoroethoxynitrobenzene are dissolved in 410 ml of tetrahydrofuran and hydrogenated at room temperature for 32 hours in the presence of Raney nickel (H2 absorption: 7.62 l). The reaction mixture is filtered and concentrated and the residue is distilled. The title compound of formula ##STR13## is obtained in the form of a colourless liquid; b.p. 56°-61° C./0.04 torr.

Provenance & Evidence