Sodium Hydroxide → HCID 178527667, compound

HRID 1650899Notes

Reaction equation

HRID 1650899 reaction equation
[C:1]([S:5]([OH:8])(=[O:7])=[O:6])([F:4])([F:3])[F:2].[OH-].[Na+:10].FF.ClCl.C(=O)([O-])[O-]>>[C:1]([S:5]([O:8][Na:10])(=[O:7])=[O:6])([F:4])([F:3])[F:2]

Participants

6

Reactant 5

HCID 14798Sodium HydroxideHCID 19660Carbonate IonHCID 24524FluorineHCID 24526ChlorineHCID 62406Trifluoromethanesulfonic acid

Product 1

HCID 178527667HCID 178527667, compound

Procedure

A teflon vessel was charged with 75% aqueous solution of CF3SO3H used in Example 1, and 50% aqueous solution of NaOH (free fluorine 33 ppm, free chlorine ppm, carbonate radical 1.1%) was poured into the solution such that the reaction between the acid and the alkali proceeded under acidic conditions and terminated while pH of the reaction liquid was 2. Then the reaction liquid was dried in the same manner as in Example 1 to thereby obtain a powder of CF3SO3Na.

Workup

  1. customterminated while pH of the reaction liquid
  2. customThen the reaction liquid
  3. customwas dried in the same manner as in Example 1

Sources & evidence

ORD record
ord-84956da50f324491ad37c4ea72c9526a
Source dataset
uspto-grants-1990_05
Patent number
US04925975

Reaction notes

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