HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 14742801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14742789 | HCID 14742789 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14742801 | HCID 14742801 | 94% |
Reaction Steps
As in Example 112, (E)-3-(1-butyl-3,4-dihydro-6-methoxy-2-naphthalenyl)-2-propenoic acid methyl ester (2.9 g) in methanol (12 mL) was treated with 2N sodium hydroxide solution (7 mL) at reflux for 1.5 hours. The usual work up provided 2.6 g of (E)-3-(1-butyl-3,4-dihydro-6-methoxy-2-naphthalenyl)-2-propenoic acid as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927838 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-3abf69727e6748f68db2dec38f799888 |
| Source note | uspto-grants-1990_05 |