2,4-Dichloro-6-nitroquinoline-3-carbonitrile → HCID 14028993, compound

HRID 1651283Notes

Reaction equation

HRID 1651283 reaction equation
[C:1]([C:3]1[C:4]([Cl:17])=[N:5][C:6]2[C:11]([C:12]=1[Cl:13])=[CH:10][C:9]([N+:14]([O-])=O)=[CH:8][CH:7]=2)#[N:2]>C1COCC1>[NH2:14][C:9]1[CH:10]=[C:11]2[C:6](=[CH:7][CH:8]=1)[N:5]=[C:4]([Cl:17])[C:3]([C:1]#[N:2])=[C:12]2[Cl:13]

Participants

3

Reactant 1

HCID 140289902,4-Dichloro-6-nitroquinoline-3-carbonitrile

Product 1

HCID 14028993HCID 14028993, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The compound was obtained by reducing 3-cyano-2,4-dichloro-6-nitroquinoline as described in Example 3. UV (THF): λmax /ε=415.2 (3,189), 304.6 (7,675), 274.0 (43,425).

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-74746a7d786848fb85aeb05ba9049a2c
Source dataset
uspto-grants-1990_05
Patent number
US04927935

Reaction notes

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