HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-aminobenzenecarbothioamide → HCID 13773249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-aminobenzenecarbothioamide | HCID 3361911 | — |
| Reactant | Benzyl glyoxylate | HCID 11008258 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13773249 | HCID 13773249 | — |
Reaction Steps
A solution of benzenecarbothioic acid hydrazide (2g) and benzyl glyoxylate (2.6g) in ethanol (5ml) was stirred at room temperature for 18 hours under nitrogen. The solvent was removed by evaporation and the residue was flash chromatographed to yield the sub-title product (3.5g) as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927822 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-ca4f184d203a4ae0bd60f177337baaad |
| Source note | uspto-grants-1990_05 |