HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl oxoacetate → HCID 23051224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | N-aminobenzenecarbothioamide | HCID 3361911 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23051224 | HCID 23051224 | 112.7% |
Reaction Steps
A solution of benzenecarbothioic acid hydrazide (0.4g) and ethyl glyoxylate (0.4g) in ethanol (1 ml) was stirred at room temperature for 2 hours. The solvent was removed by evaporation and the residue re-evaporated with toluene (x2) to yield the sub-title product (0.7g) as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927822 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-bd696e77a25c4170ada5996daf50015e |
| Source note | uspto-grants-1990_05 |