Diethyl Ether → HCID 13773300, compound

Participants

Reaction Steps

3-Acetylthiopropanoyl chloride (0.36 g), poly (4-vinyl pyridine) (0.8 g) and the product from step b) (0.8 g) were stirred together in dry toluene (30 ml) under an atmosphere of nitrogen for 20 hours. Diethyl ether was added and the solid was filtered off and washed with diethyl ether. The filtrate was evaporated under reduced pressure and the resulting product was crystallised from ethanol to yield the sub-title product (0.9 g) as a white solid. mp 120°-121°.

Provenance & Evidence