HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70364106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 14032384 | HCID 14032384 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 70364106 | HCID 70364106 | — |
Reaction Steps
A solution of 5-t-butyl-3-[N2 -(1-(S)-ethoxycarbonyl-3-phenylpropyl)-L-lysyl]-2,3-dihydro-1,3,4-thiadiazole-2-(S)-carboxylic acid (0.97 g, prepared using the appropriate starting material by the process of Example 4) in tetrahydrofuran (20 ml) and water (20 ml) was treated with 1N hydrochloric acid (3.8 ml). The solvents were evaporated and the residue was taken up in a mixture of dichloromethane and toluene. The solvents were removed by evaporation to give the title product (0.9 g) as a white
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927822 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-28bb87a4f232483596d211d7bfef4f33 |
| Source note | uspto-grants-1990_05 |