HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 13773325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 13773324 | HCID 13773324 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13773325 | HCID 13773325 | 86.1% |
Reaction Steps
A solution of the product of step (a) (1 g) in methanol (50 ml) was treated with hydrazine hydrate (0.3 g) and the mixture stirred at room temperature for 1 hour. The solvent was evaporated, the residue triturated with water, and the pH adjusted to 7 to give the sub-title product (0.8 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04927822 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-3966b38de4b84204a7f3b41a6bcef132 |
| Source note | uspto-grants-1990_05 |