HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 15611864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Butanoic acid, 2-(dimethylamino)ethyl ester | HCID 85508 | — |
| Solvent | Diisopropyl Ether | HCID 7914 | — |
| Product | HCID 15611864 | HCID 15611864 | — |
Reaction Steps
In 20 ml of isopropyl ether were dissolved 4.47 g (30 millimoles) of 2-dimethylaminoethyl butyrate ##STR8## and 3.8 g (30 millimoles) of benzyl chloride, and the solution was left to stand at room temperature for 4 days. The solvent was then evaporated. The crystals that precipitated were separated by suction filtration, washed fully with isopropyl ether, and dried under reduced pressure to give N-benzyl-N-(2-butyryloxyethyl)-N,N-dimethylammonium chloride (compound No. 29 in Table 1 given hereinbelow) represented by the following formula. ##STR9##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929267 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-1d7c8240ab4442748f4da4a6d95fdee2 |
| Source note | uspto-grants-1990_05 |