Ethyl Acrylate → HCID 53862841, compound

Participants

Reaction Steps

15.3 g of 1,3,3-trimethyl-6-aza-bicyclo[3,2,1]octane (0.15 mol) are introduced into 50 ml of diethyl ether, and 15.1 g of ethyl acrylate are gradually added thereto while stirring. A clear solution forms with a slight increase in temperature. After standing overnight at room temperature, the ether is distilled off. The oil which remains is distilled in vacuo to give 3-(1,3,3-trimethyl-6-aza-bicyclo[3,2,1]oct-6-yl)-propionic acid ethyl ester, b.p. 77°/0.013 mbar.

Provenance & Evidence