Benzoyl chloride → HCID 145809022, compound

Participants

Reaction Steps

O-phenylisourea (1 g) was dissolved in chloroform (50 ml) and triethylamine (1.2 g) and thereafter benzoylchloride (0.8 g) were added at 0° to 5° C. After stirring for one hour at 0° to 5° C., the mixture was washed with water and the chloroform was evaporated off under reduced pressure to give N-benzoyl-O-phenylisourea (1 g), m.p. 125.1° C.

Provenance & Evidence