HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14770823, compound → HCID 14770824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14770823 | HCID 14770823 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 14770824 | HCID 14770824 | — |
Reaction Steps
A solution of 0.84 g (3 mmol) of 1-acetyl-4-(4-carboxy-2,5-difluorophenyl)-1,2,3,6-tetrahydropyridine in 250 ml of acetic acid with 0.5 g of 10% Pd/c catalyst was hydrogenated at 50 psi. The title compound was isolated after filtration of the catalyst, evaporation and crystallization from acetic acid-water, mp 206°-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929613 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-15cd5ea78f534a17b5e35da1fb56bc24 |
| Source note | uspto-grants-1990_05 |