N-bromobutanimide → HCID 23050267, compound

Participants

Reaction Steps

To a stirred solution of 3-(1-hydroxyethyl)thiophene (61.4 g, 0.48 mol) in carbon tetrachloride (550 ml) was added N-bromosuccinimide (89.4 g, 0.504 mol) portionwise over 11/2 hours at 40° C. Stirring was continued for an additional 2 hours at ambient temperature. The reaction mixture was filtered and the filtrate was washed with water, saturated NaHCO3 and again with water. The solution

Provenance & Evidence