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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1651734Generated: November 2, 2026

HCID 18638260, compound → HCID 14770703, compound

https://huagongshe.com/reaction/1651734

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18638260HCID 18638260—
ReactantTrifluoroacetic acid methylene chlorideHCID 21863450—
ProductHCID 14770703HCID 14770703—

Reaction Steps

5-(N-tert-butoxycarbonyl-L-phenylalaninamidomethyl)-3-bromo-4,5-dihydroisoxazole, 7 gm, was taken in 100 ml of 20% CF3CO2H/CH2Cl2 at 0° C. for 24 hrs. Concentration gave an oily foamy substance. 1H NMR [80 MHz, CDCl3 (H2O)]; delta 2.8-3.5 (m, 4H, CH2), 4.2-4.9 (m, 2H, CH), 4.7 (s, HOD), 7.3 ppm (s, 5H, pH).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04929630
Source datasetuspto-grants-1990_05
ORD IDord-3f07533d790642ed9a09271e62f84e40
Source noteuspto-grants-1990_05