HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14848514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | 1,1,1-Tribromo-2,2,2-trifluoroethane | HCID 67718 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14848514 | HCID 14848514 | — |
Reaction Steps
83.5 g of CF3CBr3 in anhydrous DMF and 28 g of 2-chlorobenzaldehyde were reacted under a nitrogen atmosphere. The mixture was brought to 5° C. and zinc in powder (g. 16.0) was added to it slowly. Then the mixture was let reach the room temperature and kept under stirring for 6 hours. The mixture was poured into water and extracted three times with ethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929772 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-d6478588fc50402ea4ecf86ec6e72f3e |
| Source note | uspto-grants-1990_05 |