HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 14071503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | N-(2,3-Dihydro-1H-inden-2-yl)acetamide | HCID 12452137 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 14071503 | HCID 14071503 | — |
Reaction Steps
24.4 g (0.31 mol) of acetyl chloride, followed by 35.5 g (0.20 mol) of 2-acetamido-indane are added, with stirring, to a suspension of 68 g (0.51 mol) of anhydrous aluminium chloride in 350 ml of ethylene chloride. In the course of this the reaction temperature rises to approx. 50° C. Stirring is continued for a further 3 hours, the product is decomposed by means of ice and concentrated hydrochloric acid, and the organic phase is separated off and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04929754 |
| Source dataset | uspto-grants-1990_05 |
| ORD ID | ord-83c797ee24ad4f89afdc032b3324c133 |
| Source note | uspto-grants-1990_05 |