HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → Hexahelicene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 2,7-Bis(styryl)naphthalene | HCID 324155 | — |
| Product | Hexahelicene | HCID 98863 | — |
Reaction Steps
A small amount of iodine was added to a solution of 0.2 g/l of 2,7-bis(styryl)naphthalene, and the solution was irradiated with light from a high-pressure mercury lamp for 2 hr and then subjected to silica gel chromatography, and the separated product was recrystallized from benzene/ethanol as a solvent to obtain hexahelicene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05403520 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-2dfb376b25e848509513035bc1e51582 |
| Source note | uspto-grants-1995_04 |