HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15239992, compound → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15239992 | HCID 15239992 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate | HCID 15767145 | — |
Reaction Steps
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and the mixture was hydrogenated under atmospheric pressure. After completion of the reaction, the product was filtered and concentrated to obtain crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05403816 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-119bbbed187147449d212ea1efbaeb9e |
| Source note | uspto-grants-1995_04 |