HRID1653643

反应详情

EQUATION

反应方程式

HRID 1653643 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and the mixture was hydrogenated under atmospheric pressure. After completion of the reaction, the product was filtered and concentrated to obtain crystals.

WORKUP

后处理

  1. customAfter completion of the reaction
  2. filtrationthe product was filtered
  3. concentrationconcentrated
  4. customto obtain crystals