HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthalenemethanol → 5-Fluoro-3-(naphth-2-ylmethoxy)bromobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthalenemethanol | HCID 74128 | — |
| Reactant | 1-Bromo-3,5-difluorobenzene | HCID 136313 | — |
| Product | 5-Fluoro-3-(naphth-2-ylmethoxy)bromobenzene | HCID 22408606 | 92% |
Reaction Steps
Using the procedure described in the first paragraph of the portion of Example 3 which is concerned with the preparation of starting materials, 2-naphthalenemethanol was reacted with 1-bromo-3,5-difluorobenzene to give 5-fluoro-3-(naphth-2-ylmethoxy)bromobenzene (92%), m.p. 65°-67° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05403859 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-f19f9733aba84d49a5819fbe6a086129 |
| Source note | uspto-grants-1995_04 |