HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → HCID 19972716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | HCID 19972647 | HCID 19972647 | — |
| Product | HCID 19972716 | HCID 19972716 | — |
Reaction Steps
This compound was prepared by the method described for the preparation of Intermediate XVI, but using 1,5-dibromopentane in place of 1,4-dibromobutane and purifying the crude product by column chromatography on silica gel (elution with dichloromethane:ethyl acetate 99:1) m.p. 75°-76° C., after rinsing with petroleum ether:diethyl ether 30:4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05403842 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-5b38ddfa6d71440281de5db3411101d1 |
| Source note | uspto-grants-1995_04 |