Ammonium Chloride → HCID 178477983, compound

Participants

Reaction Steps

The procedure is as in Example 2, heating for 48 hours 2.4 g of 6-[4,5-bis(4-chlorophenyl)-2-oxazolyl]hexanenitrile, 1.2 g of sodium azide and 1 g of ammonium chloride in 45 cm3 of dimethylformamide. Sodium azide and ammonium chloride are added (in the same quantities as before) and the mixture is brought again to 105° C. for 48 hours. The reaction product is extracted as in the abovementioned example and crystallised in 80 cm3 of diisopropyl ether. 1.2 g of 5-{5-[4,5-bis(4-chlorophenyl)-2-oxazolyl]pentyl}tetrazole, white crystals, melting point 100° C., are obtained.

Provenance & Evidence