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HRID1653960

反应详情

EQUATION

反应方程式

HRID 1653960 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：NNc1ccc(C(F)(F)F)cc1
HCID136200

4-(Trifluoromethyl)phenylhydrazine

C7H7F3N2

结构：O=C(O)c1cccnc1C(=O)c1cccc(C(F)(F)F)c1
HCID20078895

未命名化合物

PRODUCTS

生成物

1
结构：O=c1c2cccnc2c(-c2cccc(C(F)(F)F)c2)nn1-c1ccc(C(F)(F)F)cc1
HCID20078892

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

A suspension of 2-(3-trifluoromethylbenzoyl)nicotinic acid (1.5 g) and 4-trifluoromethylphenylhydrazine (1.34 g) in toluene was stirred at reflux temperature for 3 hours (water was removed azeotropically from the mixture).

WORKUP

后处理

  1. customwas removed azeotropically from the mixture)