HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2,3-dimethylbutanamide → HCID 15672409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2,3-dimethylbutanamide | HCID 9793773 | — |
| Reactant | HCID 15672408 | HCID 15672408 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15672409 | HCID 15672409 | 128.1% |
Reaction Steps
A solution of 5-(1,3-dioxolan-2-yl)-2,3-pyridinedicarboxylic anhydride (2.64 g, 0.012 mol) and 2-amino-2,3-dimethylbutyramide (1.55 g, 0.012 mol) in tetrahydrofuran is stirred for 2 days at room temperature. The reaction mixture is concentrated in vacuo to give the title compound as an orange oil (5.4 g, 100%), identified by NMR spectra analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05405827 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-8feeeabee414483080f43813800d7387 |
| Source note | uspto-grants-1995_04 |