HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(5,6-Dimethyl-1h-benzo[d]imidazol-1-yl)butan-1-ol → 4-(5,6-Dimethylbenzimidazolyl)butylphosphoric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(5,6-Dimethyl-1h-benzo[d]imidazol-1-yl)butan-1-ol | HCID 20078957 | — |
| Reactant | Pyridinium cyanoethylphosphate | HCID 69780213 | — |
| Product | 4-(5,6-Dimethylbenzimidazolyl)butylphosphoric acid | HCID 20078961 | — |
Reaction Steps
Using 0.2 g of the crude 1-(4-hydroxybutyl)-5,6-dimethylbenzimidazole and 2 ml of 2-cyanoethylphosphoric acid pyridinium salt solution (1 mmol/ml) as the starting substances, according to the same processes as in Example 1, 0.3 g of crude 4-(5,6-dimethylbenzimidazolyl)butylphosphoric acid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05405839 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-be4113e05e574cb8aaf8816eef5ce2a0 |
| Source note | uspto-grants-1995_04 |