huagongshe.com
HRID1654083

反应详情

EQUATION

反应方程式

HRID 1654083 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1cccc(S(=O)(=O)[O-])c1.[Na+]
HCID31389

Sodium 3-nitrobenzenesulfonate

C6H4NNaO5S

结构：COc1ccc(O)cc1N
HCID20341841

3-Amino-4-methoxyphenol

C7H9NO2

PRODUCTS

生成物

1
结构：COc1ccc(O)c2cccnc12
HCID135689362

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：OCC(O)CO
溶剂HCID753

Glycerol

C3H8O3

PROCEDURE

实验过程

Following the same procedure as in Example 23-(a), reaction and treatment were carried out using 2.25 g of 3-amino-4-methoxyphenol, 3.7 ml of glycerol and sodium m-nitrobenzene sulfonate to obtain 180 mg of 5-hydroxy-8-methoxyquinoline.

WORKUP

后处理

  1. customas in Example 23-(a), reaction and treatment