HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20079018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 20079041 | HCID 20079041 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20079018 | HCID 20079018 | 98.6% |
Reaction Steps
In a mixed solvent of 10 ml of methanol and 5 ml of water were dissolved 0.55 g of 5-[N-acetyl-(2-acetoxy-3-(4-diphenylmethylpiperazine-1-yl)propylamino)]quinoline and 0.5 g of potassium carbonate, and the liquid was allowed to stand at room temperature overnight. The liquid was extracted with methylene chloride, and the extract was then dried with anhydrous magnesium sulfate and was concentrated to obtain 0.5 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05405843 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-20d067edbb4b4edea146fef2a3ab30ae |
| Source note | uspto-grants-1995_04 |