Trifluoroacetic acid → HCID 20080117, compound
Reaction equation
[CH2:1]([N:3]([CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH:25]([OH:27])[CH3:26])[CH2:4][CH2:5][CH2:6][CH:7]([C:9]1[CH:14]=[CH:13][C:12]([NH:15][S:16]([CH3:19])(=[O:18])=[O:17])=[CH:11][CH:10]=1)O)[CH3:2].FC(F)(F)C(O)=O>>[CH2:1]([N:3]([CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH:25]([OH:27])[CH3:26])[CH2:4][CH2:5]/[CH:6]=[CH:7]/[C:9]1[CH:14]=[CH:13][C:12]([NH:15][S:16]([CH3:19])(=[O:17])=[O:18])=[CH:11][CH:10]=1)[CH3:2]Participants
3
Procedure
In the process as described in Example 2 the product of Example 5 is treated with trifluoroacetic acid to give the titled compound.
Sources & evidence
- ORD record
- ord-7c76e1c1e15a41a091b6ae19bb934742
- Source dataset
- uspto-grants-1995_04
- Patent number
- US05405997
Reaction notes
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