Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Boric Acid | HCID 7628 | — |
| Reactant | HCID 86748626 | HCID 86748626 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86748625 | HCID 86748625 | — |
Reaction Steps
A solution of 1,2-dihydroxypropane octadecyl sulfide (80 g ), prepared as described in Example 1, n-butanol (43 g), and toluene (76 g) was heated to 60° C. and 9.3 g of boric acid were added. The expected amount of water was removed by azeotropic distillation with a maximum reaction temperature of 110° C. The reaction solution was filtered through diatomaceous earth. Solvent was removed by high speed rotary evaporation under reduced pressure yielding a waxy, white solid product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05407451 |
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| Source dataset | uspto-grants-1995_04 |
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| ORD ID | ord-9521fe5b28dc4ef8b03cda69d8cbbc90 |
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| Source note | uspto-grants-1995_04 |
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