HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trifluoro-2-iodoethane → HCID 20078114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trifluoro-2-iodoethane | HCID 67709 | — |
| Reactant | HCID 20078116 | HCID 20078116 | — |
| Product | HCID 20078114 | HCID 20078114 | 61% |
Reaction Steps
Using a similar procedure to that described in Example 1, 4-mercapto-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran was reacted with 2,2,2-trifluoroethyl iodide to give 4-[3-(naphth-2ylmethoxy)phenyl]-4-(2,2,2-trifluoroethylthio)tetrahydropyran in 61% yield, m.p. 76°-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05407945 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-b55c0665be7e4a5780771a52829f719f |
| Source note | uspto-grants-1995_04 |