HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20078495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 4-[2-(4-cyanobenzenesulphonylamino)-ethyl]-cyclohexylacetate | HCID 20078478 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20078495 | HCID 20078495 | 72% |
Reaction Steps
by saponification of the ethyl 4-[2-(4-cyanobenzenesulphonylamino)-ethyl]-cyclohexylacetate with 2N sodium hydroxide solution in ethanol analogously to EXAMPLE 2c). Yield 72% of theory; m.p. 172-174° C. after recrystallisation from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05407951 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-d1ecf1725ae648b78b23a25243b84156 |
| Source note | uspto-grants-1995_04 |