反应详情

温度

0 °C

4-benzylbenzyl alcohol (181.47 g) was dissolved into chloroform (100 ml), and thionyl chloride (66.8 ml) was added with stirring at a 0° C. After stirring at 0° C. for 4 hours, reaction mixture was concentrated under reduced pressure to give the title compound (198.34 g). This product was used in the subsequent procedure without purification.

1. additionwas added
2. stirringAfter stirring at 0° C. for 4 hours
3. customreaction mixture
4. concentrationwas concentrated under reduced pressure