Thionyl Chloride → Benzene, 1-(chloromethyl)-4-(phenylmethyl)-

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

4-benzylbenzyl alcohol (181.47 g) was dissolved into chloroform (100 ml), and thionyl chloride (66.8 ml) was added with stirring at a 0° C. After stirring at 0° C. for 4 hours, reaction mixture was concentrated under reduced pressure to give the title compound (198.34 g). This product was used in the subsequent procedure without purification.

Herkunft & Nachweise