HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 20076787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 15287725 | HCID 15287725 | — |
| Product | HCID 20076787 | HCID 20076787 | 87% |
Reaction Steps
4.7 g of 1-cyclopropyl-6-fluoro-7-(4-t-butoxycarbonylpiperazin-1-yl)-3-(2-nitroacetyl)-1,4-dihydro-4-oxoquinoline obtained from Example 3 was dissolved in 20 ml of trifluoroacetic acid and then stirred for 10 minutes. The solvent was removed, and the solid formed after addition of 50 ml of acetone was filtered and then dried to obtain 4.25 g of the object compound
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409933 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-168dc9b8e1554d0799aaae58fe0aa00b |
| Source note | uspto-grants-1995_04 |