Water → HCID 15278048, compound

HRID 1654810Notes

Reaction equation

HRID 1654810 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][C:11]=1[Cl:12])[O:5][CH2:6][CH2:7]Br.C(=O)([O-])[O-].[Na+].[Na+].[CH2:19]([NH2:27])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].O>C(O)C>[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][C:11]=1[Cl:12])[O:5][CH2:6][CH2:7][NH:27][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

6

Reactant 4

HCID 962WaterHCID 8143OctylamineHCID 10340Sodium CarbonateHCID 2807934-(2-bromoethoxy)-1,2-dichlorobenzene

Product 1

HCID 15278048HCID 15278048, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In 20 ml of ethanol was dissolved 2.06 g (7.63 millimoles) of 2-(3,4-dichlorophenoxy)ethyl bromide, and 1.06 g (10.0 millimoles) of anhydrous sodium carbonate and 3.48 g (27.0 millimoles) of n-octylamine were added to the solution. The mixture was heated and refluxed on an oil bath for 6 hours. After cooling, the reaction mixture was poured into 100 ml of water and extracted with 20 ml of chloroform three times.

Workup

  1. additionwere added to the solution
  2. temperatureThe mixture was heated
  3. temperaturerefluxed on an oil bath for 6 hours
  4. temperatureAfter cooling
  5. extractionextracted with 20 ml of chloroform three times

Sources & evidence

ORD record
ord-4d02161100a64d19b44ead58151728a2
Source dataset
uspto-grants-1995_04
Patent number
US05409957

Reaction notes

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