Water → HCID 15278048, compound

Participants

Reaction Steps

In 20 ml of ethanol was dissolved 2.06 g (7.63 millimoles) of 2-(3,4-dichlorophenoxy)ethyl bromide, and 1.06 g (10.0 millimoles) of anhydrous sodium carbonate and 3.48 g (27.0 millimoles) of n-octylamine were added to the solution. The mixture was heated and refluxed on an oil bath for 6 hours. After cooling, the reaction mixture was poured into 100 ml of water and extracted with 20 ml of chloroform three times.

Provenance & Evidence